R-301 Series   Catalyst Pilot Plant System

  Catalyst Pilot Plant System

 Gas Feed Module

 Liquid Feed Module

 Preheater Module

 Reactor Module

 Separator Module

 Receiver Tank Module

 Gas Product Module

 Super Kanthal High Temp. Tubular Furnace

 R-301 Series Tubular Reactor

 T-301 Series Feed Tank

 Electric Heaters

Catalyst Pilot Plant System

Use of Catatest
 
-  Determinations of different variables for researching on Catalyst improvement, such as; Reacting Temperature,
   Pressure and Feed Flow, etc.
-  Test of Catalyst on Hydrogen reaction
-  Catalyst Screen, Selectivity & Activity Test
-  Test of Catalyst Life Span
 
Guideline for Process Design
 
-  Catalyst volume (5ml ~ 2 liter)    : 316SS & Hastelloy.C-276
-  Reactor design pressure              : 1000 psig ~ 6000 psig
-  Reactor design temperature : 800'C
-  Operating temperature : 650'C
-  Operating pressure : 1200 psig
-  Liquid viscosity : 40 cp Max. (at pump after heating)
-  Liquid flow range : 20ml/min ~ 100 liter/min
-  Gas flow range : H2 : 50ml/min ~ 3 liter/min
                              O2 : 50ml/min ~ 3 liter/min
                              N2 : 50ml/min ~ 500ml/min
                              Feed & spare : 50ml/min ~ 500ml/min
 
Composition of Catatest
 
-   Gas feed module
-   Liquid feed module
-   Reactor
-   Gas product module
-   Liquid product module
-   Steam feed module
 
On Material, Fitting, Valve & Tubing
 
-  316 Stainless steel & Hastelloy.C-276
-  Fitting and Valve will be used of BuTech, Hoke, Swagelok made, however, customers' request for using
   other makers are also acceptable.
-  Valve for Catatest B/L should be used only of BuTech made.
 
 
Gas Feed Module
 
Purpose of having this module
 
-   For supplying with fixed amount of Feed and Flow into the Reactor for the High pressure gas cylinder.
    cf. Figure : Mass Flow Controller (FCV-301)
   
Condition
-  Accurate Gas Flow control must be performed.
-  Accurate Gas Pressure control must be performed.
-  Pressure safety valve should be attached.
-  Filtering should be available.
-  An immediate action should be able to be taken for unexpected Emergency.
-  H2 & Air line shouldn't be used at the same time.
   
Gas Material
Flow Range
Max Pressure
H2
O2
N2
Feed & Spare
50ml/min ~ 3 liter/min
50ml/min ~ 3 liter/min
50ml/min ~ 500ml/min
50ml/min ~ 500ml/min
6000 psig
6000 psig
6000 psig
6000 psig
 
 
Specification
-  Gas flow range and Max pressure
-  Number of Feed line : 4 Lines (H2, O2, N2, Feed & Spare)
 
Compositions
-  Pressure control valve
-  Mass flow control valve
-  Pressure safety valve
-  Solenoid valve
-  Filter
-  Check vlave
-  Block valve
-  Pressure indicator & Transmitter
 
Liquid Feed Module
 
Purpose of having this Module
 
-  Supplying with Liquid feed under fixed pressure and temperature into the System.
     cf. Figure : Metering Pump (P-301) , Feed Tank (T-301)
 
Conditions
- Accurate Flow control of Liquid feed is a must.
- Accurate Pressure control of Liquid feed is also a must.
- Pressure safety valve must be installed.
- Filtering should be available.
- An immediate action must be able to be taken for unexpected Emergency.
- Fixed temperature for Liquid feed should be maintained.
- Electronic tracing must be available for keeping the Line temperature control.
- Liquid feed inside the Tank must not be contacted with air.
- Tank will be used for Sampling bottle.
 
Specification
 
-  Liquid feed rate : 5ml/min ~ 1 liter/min
-  Viscosity : 40 cp
-  Capacity : 2 liter ~ 10 liter
-  Design Pressure : 6000 psig
-  Pump (Eldex, Milton Roy)
      1) Metering pump
      2) Max temperature : 50'C
-  Numbers of Tank : 2 (including 1 spare tank)
 
Compositions
 
-  Liquid feed tank : Includes Temperature Controller
-  Agitator
-  Filter
-  Feed line's temperature will be controlled by electronic tracing
   Pressure safety valve
-  Check valve
-  Drain valve
-  Block valve
-  Metering pump
-  Weigher
-  Three-way valve
-  Pressure control valve
-  Line filter
-  Pressure gauge (Indicator)
 
Preheater Module
 
Purpose
 
-  For Mixing and Preheating of Reactant
     cf. Figure : Furnace (5-Zone) : H-301
 
Conditions
 
-  Temperature in the Preheater / Furnace should be auto-controlled.
-  Pressure safety valve must be installed.
-  Electronic tracing should be available for temperature control in the outlet line of Preheater.
-  No 'flow hunting' by Preheater is allowed in no case.
 
 
Specification
 
-  Max temperature : 800'C
-  Max pressure : 6000 psig
-  Materials : 316SS & Hastelloy.C-276
 
Compositions
 
-  Pressure safety valve
-  Furnace (5-Zone)
-  Pressure safety element
-  Check valve
-  Temperature element (For TIC control)
-  Electronic tracing should be available for temperature control in the Outlet line of Preheater.
 
 
Reactor Module
 
Purpose
 
-  To get the Reactions of preheated feed from the Reactor's Catalyzer of the Preheater.
     cf. Figure : Furnace (5-Zone) : H-301
 
Conditions
 
-  Max temperature of Furnace : 800`C
-  Using 5 different Sensors on the Furnace, the Furnace shall be TIC temperature controlled to show 5 different areas'    temperatures constantly. If/When any one area of the 5 parts shows exceeding temperature than standard, Power to the    Furnace will be shut down immediately and, Solenoid valve of Feed line will be closed while Outlet solenoid valve and    Nitrogen solenoid valve will be opened up.
-  Pressure safety valve and Pressure safety element shall be installed.
-  By the same way as above, temperature inside the Reactor will be controlled in 4 different area, and if/when any one area
   shows exceeding temperature the same actions as above will be taken immediately.
-  System pressure control : Under normal situation, pressure can be controlled either by pressure before preheated or    Reactor's outlet pressure. For an emergency, System can be controlled by Preheater inlet pressure because even though    Reactor's outlet solenoid valve was opened it doesn't help any.
 
Specification
 
-  Catalyst volume : 5ml ~ 2 liter
-  Max pressure : 1000 psig ~ 6000 psig
-  Max temperature : 800'C
-  Operating temperature : 650'C
-  Operating pressure : 2000 psig
-  Capacity of Reactor : 5ml ~ 2 liter
-  Type of Reactor : Tubular fixed bed reactor for both up or down flow as required for process
 
Compositions
 
-  Furnace (5-Zone)
-  Reactor
-  Solenoid valve
-  Block valve
-  TIC temperature controller
 
 
Separator Module
 
Purpose
 
-   Cooling of Effluent gas, and separation of Gas and Liquid
      cf. Figure : Separator (S-301)
 
Conditions
 
-  Cooling water should be used for Condenser
-  Condenser line to be installed
-  By-pass valve to be installed for Separator's liquid level control for an emergency case in the level control valve
-  No 'Flow hunting' by Condenser is allowed in no case
 
Specification
 
-  Max temperature : 250'C
-  Max pressure : 2000psig
 
Compositions
 
-  Condenser
-  High pressure separator
-  Level gauge
-  Level control valve
-  Condenser by-pass line (valve)
-  Block valve
-  Glove valve
 
 
Receiver Tank Module
 
Purpose
 
-  Liquid product receiving
      cf. Figure : Receiver Tank (T-301)
 
Conditions
 
-  Receiver weighing
-  Direct sampling from Receiver
-  Gas produced from the Receiver should be connected through entire gas meter
 
  
Compositions
 
-  Product receiver
-  Weigher
-  Drain valve
-  Sampling valve
 
 
 Gas Product Module
 
Purpose
 
-   Ventilation of Gas product. Some of them shall be G/C constituent analyzed.
      cf. Figure : Condenser (Shell & Tube Type)
 
Conditions
 
-  The entire System should be pressure controlled.
-  Pressure in G/C line to be maintained uniformly.
-  Sampling by syringe should be available.
-  Pressure safety valve to be installed.
-  Gas meter to be installed for measuring Gas amount.
 
Compositions
 
-  Filter
-  Gas meter
-  Pressure control valve
-  Pressure safety valve
-  G/C line solenoid valve
 
 
  Super Kanthal High Temp. Tubular Furnace
 
General Information
 
-  Our Model H-301 series Electric Furnace can be used under high temperature. As the Model has High Al2O3 Tube installed     inside, ambience control for the system use is available, and the diameter and length of the Tube can be selected as users     wants.
 
 
Features
 
-  Various different size of Tubes are welcome to use
-  Ambience use is available
-  While using Ambience, Redox and changing of Neutral ambience is also available
 
Specification
 

Model

H-301

H-302

H-303

I. D.

60mm

80mm

100mm

Max Temperature

1800'C

1800'C

1800'C

Power

220VAC, 1Ph

220VAC, 1Ph

220VAC, 1Ph

Atmosphere

Oxidization, Deoxidization

Temp. Controller

P. I. D. Programmable controller

 
 
Applications
 
-  Chemical : Hydrogenation, Selective Oxidation, Ammoxidation, Isomerization
-  Petroleum : Cracking, Hydro-cracking, Hydro-processing, Isomerization, Reforming
-  Environmental : Liquid waste disposal Total oxidation Effluent treatment Resource conservation
 
 
R-301 Series Tubular Reactor
 
The Tubular Reactor is packed with solid catalyst particles. The straight through flow of gases and/or liquids high conversion levels.
    Reactant : Liquid / Solid
                     Gas / Solid
                     Gas / Liquid / Solid
    Applications : Hydrogenation, Oxidation, hydrotreating, Catalyst testing
    Materials : 316SS and Hastelloy.C-276, Titanium
    Max. Pressrue : 6,000 psig at 800'C
     cf. Figure :  Tubular Reactor (R-301)
 
Ordering Information
 

Model No.

Capacity

Design Pressure

Design Temp.

Materials

Outside Dia.

Outside Dep.

Connections

R-301-8

8ml

6000 psig

800'C

316SS & Hast.C-276

3/8"

200mm

1/8"NPT(F)

R-301-12

12ml

6000 psig

800'C

316SS & Hast.C-276

3/8"

300mm

1/8"NPT(F)

R-301-16

16ml

6000 psig

800'C

316SS & Hast.C-276

1/2"

200mm

1/8"NPT(F)

R-301-24

24ml

6000 psig

800'C

316SS & Hast.C-276

1/2"

300mm

1/8"NPT(F)

R-301-160

160ml

6000 psig

800'C

316SS & Hast.C-276

1"

300mm

1/4"NPT(F)

R-301-380

380ml

6000 psig

800'C

316SS & Hast.C-276

1"

500mm

1/4"NPT(F)

R-301-590

590ml

6000 psig

800'C

316SS & Hast.C-276

2"

300mm

1/4"NPT(F)

R-301-980

980ml

6000 psig

800'C

316SS & Hast.C-276

2"

500mm

1/4"NPT(F)

 
 
T-301 Series Feed Tank
 
-  Design Pressure : 5000 psig
-  Design Temperature : 250'C
-  Materials : 316SS & Hastelloy.C-276
     cf. Figure : Feed Tank (T-302
 
Ordering Information
 

Order No.

Capacity

Pressure

Dimensions (mm)

A

B

C

D

E

   T-301-SS3

        300ml

2000 psig

111

220

71

51

150

   T-301-SS5

        500ml

2000 psig

115

300

75

55

230

   T-301-SS1

      1000ml

2000 psig

146

250

108

86

180

   T-301-SS2

      2000ml

2000 psig

154

350

118

94

280

   T-301-SS4

      4000ml

1000 psig

187

400

155

127

330

   T-301-SS8

      8000ml

1000 psig

215

530

185

155

460

   T-301-SS10

    10000ml

1000 psig

263

654

233

203

584

 
 
 Electric Heaters
 
HT Series Ultra High Temperature Semi-Cylindrical Helically Wound Ribbon Ceramic Heaters
 
-  Helically Wound Ribbon Iron-Chrome-Aluminum
-  Rated to 2192'F (1200'C)
-  Low Mass Vacuum Formed Ceramic Fiber
-  Use Two Semi-Cylindrical Units to Form a Full Cylinder
 
Applications for HD Models
 
-  Pipe Heating
-  Process Air Heating
-  Calibration Ovens
-  Strain Annealing Ovens
-  Tube Furnace
-  "B" Type Thermocouple
  
Without Vestibules
With the HT Series the helically wound iron-chrome-
Aluminum ribbon elements are mounted in ridges which
premits heat dissipation in three directions, thereby
transferring more radiant heat energy to work
With Vestibules
Chamber and load. Using this design effectively triples
the radiant heating surface. The unique design allows for
two semi-cylindrical units to be combined to form a full
cylinder heating element.
 
Specifications
 
            Semi-Cylindrical Helically Wound Ribbon Models
            Wattage : 800 to 9500 Watts
            Voltage  : 110 & 220 VAC Single and Dual Circuits
 

Model Number : HT Series Semi-Cylindrical Helically Wound Ribbon Models

Watts

 Volts

A DIM*      B DIM       C DIM        D DIM

Without Vestibules

With Vestibules

Dimensions are in inches

Model Number

Model Number

1600

220

            12              11              7                5

HT-127/220

HT-127/220

2400

220

            18              11              7                5

HT-187/220

HT-187/220

3200

220

            24              11              7                5

HT-247/220

HT-247/220

1800

220

            12              12              8                6

HT-128/220

HT-128/220

2700

220

            18              12              8                6

HT-188/220

HT-188/220

3600

220

            24              12              8                6

HT-248/220

HT-248/220

2250

220

            12              14              10              8

  HT-1210/220

  HT-1210/220

3375

220

            18              14              10              8

  HT-1810/220

  HT-1810/220

4500

220

            24**           14              10              8

  HT-2410/220

  HT-2410/220

2700

220

            12              16              12              10

  HT-1212/220

  HT-1212/220

4050

220

            18              16              12              10

  HT-1812/220

  HT-1812/220

5400

220

            24**           16              12              10

  HT-2412/220

  HT-2412/220

3400

220

            12              19              15              13

  HT-1215/220

  HT-1215/220

5100

220

            18              19              15              13

  HT-1815/220

  HT-1815/220

6800

220

            24**           19              15              13

  HT-2415/220

  HT-2415/220

4100

220

            12              22              18              16

  HT-1218/220

  HT-1218/220

6150

220

            18              22              18              16

  HT-1818/220

  HT-1818/220

8200

220

            24**           22              18              16

  HT-2418/220

  HT-2418/220

4750

220

            12              25              21              19

  HT-1221/220

  HT-1221/220

7125

220

            18              25              21              19

  HT-1821/220

  HT-1821/220

9500

220

            24**           25              21              19

  HT-2421/220

  HT-2421/220

 
* Add 3" for units with vestibules
** Using two 12" long heaters; the indicated wattage is the total of twc 12" long heaters.
 
Ordering Information
 

301

A

B

C

D

E

F

G

 

  Capacity

Pressure

 Temp.

   Power

   Catalyst Baskets

   Control System

 MFC

 Series
  301
1 :     8ml
2 :   12ml
3 :   20ml
4 :   50ml
5 : 100ml
6 : 150ml
7 : 300ml
8 : 500ml
9 : Other
1 :   300 psig
2 :   500 psig
3 : 1000 psig
4 : 1500 psig
5 : 2000 psig
6 : 3000 psig
7 : 5000 psig
8 : Other
1 : 300 `C
2 : 400 `C
3 : 500 `C
4 : 600 `C
5 : 700 `C
6 : 800 `C
7 : Other
1 : 110/60/1
2 : 220/60/3
3 : 330/60/3
4 : Other
1 : 5ml
2 : 10ml
3 : Other 
1: PLC
2 : DCS
3 : Other
1 : MFC(1)
2 : MFC(2)
3 : MFC(3)
4 : MFC(4)
5 : MFC(5)
6 : Other
 Send your inquiryInquiry form
 E-mail: lab@labkorea.com
ESEL TechTra Inc.
 #1382-4, Kuweol-3dong, Namdongku, Incheon, korea
 ¨ÏCopyright 1999 www.labkorea.com ® All right reserved